WebSPE) was performed on FluoroFlash 2 g cartridges as follows: The cartridges were preconditioned with 1 mL N,N-dimethylformamide (DMF) and 7 mL 80:20 MeOH/H 2O, loaded with the crude alkylation reaction mix-ture, washed with 7 mL 80:20 MeOH/H 2O, and eluted with 10 mL MeOH. Each F-SPE cartridge was used only once. WebMar 26, 2024 · After the addition of FluoroFlash® (2.6 g, 30 times the weight of the catalyst) to the reaction mixture, 3 mL of water (same of the volume of toluene) was added, and the mixture was stirred for 15 min. The subsequent filtration of the reaction mixture afforded the catalyst 1a in an immobilized form. Further, the filtrate was subjected to ...
Versatile synthesis of probes for high-throughput enzyme
Webor R 1 and R 2, together with the phenyl ring to which they are attached, combine to form a 2,3-dihydro-benzo[b]thiophene, 2,3-dihydro-benzo[b]thiophene 1-oxide, 2,3-dihydro-benzo Web111003579 Print MilliporeSigma™ Supelco™ FluoroFlash™ SPE Cartridges Solid phase extraction (SPE) is a technique commonly used in laboratories to isolate analytes of … how do undersea earthquakes cause tsunamis
Fluorous parallel synthesis of a hydantoin/thiohydantoin library
WebThe present invention relates to compositions and methods for treating a disease in an animal, which disease is responsive to inhibiting of functional cystic fibrosis transmembran WebJul 1, 2003 · The product purification is performed by solid-phase extraction over FluoroFlash cartridges, and no fluorous solvent is involved in either the reaction or the separation processes. The same method applies to synthesis of thiohydantoins. ... The cartridge was eluted with 10–15 mL of 80:20 MeOH/H 2 O. The fraction was collected … WebApr 1, 2004 · Fluorous synthesis unites the attractive features of solution-phase chemistry with the convenient workup of solid-phase chemistry. 8 Molecules attached with a perfluoroalkyl “phase tag” can be easily isolated from the reaction mixture by fluorous separation techniques such as fluorous solid-phase extraction (F-SPE). 9 The fluorous … how much snow in ridgewood nj